Carnegie Mellon

NSF Grant DMR 0520425

High School Teachers Summer Internship

 

 

 

 

 

 

 

Introduction

As a marble and granite fabricator it was very advantageous to determine when a material would fail.  Hopefully this determination could be made prior to investing in a finished, polished piece.  Failure of the material was often catastrophic and befuddling.  There was a very strong motivation to anticipate these failures because although the material was expensive the labor involved in finishing a piece was the primary investment.  As a fabricator several rules of thumb developed.  Granite was much more consistent, reliable and stronger than marble.  Marbles might be very strong in their primary composite, however, they almost always failed along their veining.  Granite was many times stronger that granite ( I believed about ten times stronger, and it took 10 times the grit to polish:  220-600 grit for marbles, whereas it was 3,000-5000 grit for granites).  Dark stones also were stronger than lighter stones.

 

 

 

 

 


 

 


 

Carnegie Mellon

NSF Grant DMR 0520425

High School Teachers Summer Internship

 

 

 

 

 

 

 

Objective

The goal of this research project, as a high school physics teacher, was to test these pragmatic assumptions and to attempt to quantify the relative strengths of marble and granite.  I determined to do a 3-point flexure test (known as modulus of rupture test, ASTM C880-06) because the stone usually failed under tensile forces.  I also conducted compressive tests to determine what I expected was the relative true strength of the material.  I also conducted Zwick hardness tests to determine the variability of relative hardnesses between samples and within samples.  In the course of e vents I ended up utilizing a SEM (scanning electron microscope) in an attempt to understand my results related to the grain size, flaw size and fracture propagation.  I also looked at x-ray diffraction in the granites to attempt to understand the relative strengths and weaknesses in the small grained and large grained granite.

I chose seven samples.  I used tile because it was pre-polished, regular and easily prepared for consistent samples and the 1 cm thickness, I believed, was in the strength range that I could test with the testing equipment available to me. I chose a white and black marble, the whitest granite that I could find, an equally small grained pure black granite, a larger grained white granite of apparently similar composition to the light granite, a yellow marble that had significant white “inclusions” that I expected would act as natural flaws and provide the weakest sample, and as a last sample I chose a dark granite with obvious differences in composition to test the further effect of different potential “grain” boundaries.  I cut all of the samples out of single tiles so that there was a consistency of material.  Thus the samples were all out of the same batch and were located immediately adjacent to each other.  Although the rift of the stone could not be determined on such small samples, this method determined the rift of the individual samples to all be the same and insured as much consistency among naturally variable materials as possible.  The variability of natural stone was a huge aspect of this experiment and it was my intention to limit that variability as much as possible.

 

 

 

 

 


 

 

 

Carnegie Mellon

NSF Grant DMR 0520425

High School Teachers Summer Internship

 

 

 

 

 

 

 

Background

 

Stone is a naturally variable material and it is classified as a brittle material.  A brittle material is one that fractures rather than deforms significantly under stress.  In the material science text book, Elements of Materials Science and Engineering, it indicates that “The ultimate mechanical failure is fracture.  We commonly categorize fracture as being either ductile or brittle (i.e. nonductile)…Brittle fracture requires energy to separate atoms and to expose new surface along the fracture path.” ( Van Vlack, 1989)  I tested the compressive and tensile strength of the stone.  Stone is known to have a very high compressive strength.  Compressive strength is determined by putting a material under a load which results in compressive stress on the material.  A brittle material under compressive strength deforms little and results in fracture when the tensile stress that attempts to deform the material outward exceeds the molecular strength of the material to maintain its structure.  This is associated with the angle of friction at which the materials fail under compressive load.  The 3-point flexure test supports the material at its ends and submits the sample to the load in the middle.  This causes a compressive stress on the top and a tensile strength on the bottom of the sample.  Since stone has a much higher compressive than tensile strength, the sample will fail much sooner in the flexure test, and will fail from the bottom of the sample to the top.

 

Marble is formed by a metamorphic process.  This means that sedimentary or disintegrated material is put under pressure and heat by being deeply buried under ground for a long period of time.  The pressure and heat transform the crystalline structure.  The bonding material, which is considerably weaker, gradually becomes a crystal structure that increases in hardness and strength.

 

Granite is an igneous material, meaning that it is formed by magma or lava.  The slower the lava cools the larger the crystals that form.  From experience and from my research on flaw sizes, I believed that larger grained granites would be weaker than smaller grained granites.  Larger grains created the beginnings of larger flaws that would more readily propagate in the various samples.

 

For my samples I chose a light and black marble and granite.  In the granites I chose small grained granites for consistency in these samples.  I also chose a large grained white granite with similar coloration of the smaller grained light granite for comparison.  In the marble, instead of a grain size I chose a black marble with pronounced white veining, which I considered a natural flaw, and I chose a yellow marble which looked a lot like a non-metamorphic travertine, which I thought with its variability would be my weakest sample of all.

 

Van Vlack, Lawrence H. Elements of Materials Science and Engineering.  Sixth Edition.     Addision-Wesley Publishing Company. New York.  1989.

 

 

 

 

 


 

 

 

Carnegie Mellon

NSF Grant DMR 0520425

High School Teachers Summer Internship

 

 

 

 

 

 

 

What will you Need?

 

I did additional test, including a Vickers hardness test, SEM analysis of the fracture surface and x-ray diffraction analysis of the granite chrystaline structure, however, these tests are not part of the designed lab.

 

For the lab, the students will conduct a 3-point flecture test (modulus of rupture, modified ASTM  888-90), and a compression test (modified ASTM 170-08).  The modifications to the ASTM standard tests are to maintain the dimensions of the samples proportionally but reducing all dimensions so that they are manageable for testing in the high school laboratory.)

 

For both tests the students will need :

  • Steel Frame rated for a 10 ton load
  • Hydraulic cylinder and pump rated at 10 tons (limit for compression test to achieve 29,000 psi)
  • 3-point flexure apparatus
  • 1 inch steel compression plate machined to fit piston
  • 3 – 3”x1”x3/8” samples of each stone (per class) each team does one sample  (7 groups with 3-4 students each)
  • 10 – 3/8” cubes of each stone sample (per class); 7 groups each do 10 samples of one stone
  • 1 – video capable camera

 

 

 

 

 

 


 

 

 

 

Carnegie Mellon

NSF Grant DMR 0520425

High School Teachers Summer Internship

 

 

 

 

 

 

 

Procedures:

 

3-Point Flexure Test – SAFETY FIRST!!!

 

1.      Set up the frame and 3-point apparatus

2.      Make sure that the apparatus and sample are centered

3.      Place the safety shield in front of the frame (in between you and the frame)

4.      Slowly engage the hydraulic piston until it is almost touching the sample

5.      Begin videoing the gauge

6.      Slowly pump up the pressure

7.      Stop applying the pressure when the sample fails (there wil be an abrupt drop in pressure- a dramatic failure!)

8.      Rewind the viedo and record the maximum pressure on the gauge

9.      Release the pressure

10. Remove the safely shield

11. Draw a picture of the sample as it is after the failure.

12. Remove the sample

13. Repeat step 1-12 for each sample

 

Compression Test- SAFETY FIRST!!!

 

The procedure for the compression test is the same as for the 3 point flexure test escept for step 1:

 

  1. Set up the compression fitting on the steel frame
  2. complete steps 2-13 of the procedure above

 

 

 

 

 

 


 

 

 

Carnegie Mellon

NSF Grant DMR 0520425

High School Teachers Summer Internship

 

 

 

 

 

 

Lesson Plans

 

Introductory Set:  Stone has been utilized as a building material for thousands of years.  There are many reasons that stone has been used so pervasively, but for our purposes today we would like to concern ourselves with the properties of strength that make stone such a good building material.  When we talk about strength in stone we are referring to the materials ability to withstand applied forces.  The applied forces, in our case called load, result in compression and tensile stresses.  Compression stresses are forces that push materials together and tensile stresses are forces that tear materials apart.  In the next few days we will be considering and testing both compression and tensile stresses on different types of stone.  For our purposes we will be considering two different types of stone:  marbles and granites.  Marbles are a metamorphic material resulting from materials being formed under heat and pressure from being buried under ground for a long period of time.  Granites, which often have a speckled appearance, are called igneous and are the result of lava cooling at different rates.  What we would like to find out is, How strong are marbles and granites relative to each other and to different samples of the same type?  And How much variability is there in the strength of these natural materials due to natural variability?

 

So our goal is to determine the relative strength of 7 different samples of stone: 3 marbles and 4 granites.  In the end as a class we will attempt to answer the questions, Are marbles or granites stronger? And can we ascertain from a particular sample whether it will be able to sustain a greater load than another sample of a different stone or even the same stone?  Given this analysis we will attempt to discuss what variability among natural materials means within a scientific experiment and how we can design a lab so that we can address this variability.

 

So now let’s get out our lab notebooks and begin testing!  Using the scientific method make a hypothesis about which of the seven samples you believe will be the strongest and why.  Also answer the question whether the strength of the materials will be the same under compression and under the 3-point tensile test.  Which test do you suspect will result in higher load strengths?

 

Now we are ready to begin.  You will conduct compression and tensile strength tests.  Compression tests apply stresses that force a material together, whereas tensile stresses pull a material apart.  In stone, do you expect the strength to be greater in compression or tension?

 

Let’s find out!  Begin the procedure for the 3-point flexure test.  Then complete the compression test.  Carefully document all of your results including your drawings.

 

Begin conducting the lab.  Safety First!  If you have any questions ask the teacher and document all of your questions and findings.

 

When the Lab is completed…

 

Share your data with the class.  This will give us a larger data set.  How does this help address the natural variability of our samples.  What did you find?

 

Write up a lab report about your findings.  Make graphs of your findings. What conclusions can you draw about the relative strengths of the different stones?  Are you convinced that your findings are accurate?  How would you continue this laboratory exploration?

 

Educational Standards Used and/ or Met

 

Content Standard A: Science As Inquiry

A1: Abilities necessary to do scientific inquiry:

  • Identify questions and concepts that guide scientific investigations
  • Design and conduct a scientific investigation
  • Use technology and mathematics to improve investigations and communications
  • Formulate and revise scientific explanations and models using logic and evidence
  • Recognize and analyze alternative explanations and models
  • Communicate and defend a scientific argument

 

A2: Understanding about scientific inquiry:

  • Scientists usually inquire about how physical systems function
  • Scientist conduct investigations for a wide variety of reasons
  • Scientists rely on technology to enhance the gathering and manipulation of data
  • Mathematics is essential in scientific inquiry
  • Scientific explanations must adhere to criteria such as a proposed explanation must be logically consistent; it must abide by the rules of evidence; it must be open to questions and possible modifications; and it must be based on historical and current scientific knowledge
  • Results of scientific inquiry emerge from different types of investigations and public communications among scientists

 

Content Standard B: Physical Science

B2: Structure and properties of matter

 

Content Standard G: Science as Inquiry

G1. Science as a human endeavor:

  • Individuals and teams have contributed and will continue to contribute to the scientific enterprise
  • Scientists have ethical traditions
  • Scientists are influenced by societal, cultural, and personal beliefs and ways of viewing the world

 

G2. Nature of scientific knowledge

  • Science distinguishes itself from other ways of knowing and from other bodies of knowledge
  • Scientific explanations must meet certain criteria
  • Because all scientific ideas depend on experimental and observational confirmation, all scientific knowledge is, in principle, subject to change as new evidence becomes available

 

 

 

 

 

 

 

 

Carnegie Mellon

NSF Grant DMR 0520425

High School Teachers Summer Internship

 

 

 

 

 

 

 

Lesson Plans

Introductory Set:  Stone has been utilized as a building material for thousands of years.  There are many reasons that stone has been used so pervasively, but for our purposes today we would like to concern ourselves with the properties of strength that make stone such a good building material.  When we talk about strength in stone we are referring to the materials ability to withstand applied forces.  The applied forces, in our case called load, result in compression and tensile stresses.  Compression stresses are forces that push materials together and tensile stresses are forces that tear materials apart.  In the next few days we will be considering and testing both compression and tensile stresses on different types of stone.  For our purposes we will be considering two different types of stone:  marbles and granites.  Marbles are a metamorphic material resulting from materials being formed under heat and pressure from being buried under ground for a long period of time.  Granites, which often have a speckled appearance, are called igneous and are the result of lava cooling at different rates.  What we would like to find out is, How strong are marbles and granites relative to each other and to different samples of the same type?  And How much variability is there in the strength of these natural materials due to natural variability?

 

So our goal is to determine the relative strength of 7 different samples of stone: 3 marbles and 4 granites.  In the end as a class we will attempt to answer the questions, Are marbles or granites stronger? And can we ascertain from a particular sample whether it will be able to sustain a greater load than another sample of a different stone or even the same stone?  Given this analysis we will attempt to discuss what variability among natural materials means within a scientific experiment and how we can design a lab so that we can address this variability.

 

So now let’s get out our lab notebooks and begin testing!  Using the scientific method make a hypothesis about which of the seven samples you believe will be the strongest and why.  Also answer the question whether the strength of the materials will be the same under compression and under the 3-point tensile test.  Which test do you suspect will result in higher load strengths?

 

Now we are ready to begin.  You will conduct compression and tensile strength tests.  Compression tests apply stresses that force a material together, whereas tensile stresses pull a material apart.  In stone, do you expect the strength to be greater in compression or tension?

 

Let’s find out!  Begin the procedure for the 3-point flexure test.  Then complete the compression test.  Carefully document all of your results including your drawings.

 

Begin conducting the lab.  Safety First!  If you have any questions ask the teacher and document all of your questions and findings.

 

When the Lab is completed…

 

Share your data with the class.  This will give us a larger data set.  How does this help address the natural variability of our samples.  What did you find?

 

Write up a lab report about your findings.  Make graphs of your findings. What conclusions can you draw about the relative strengths of the different stones?  Are you convinced that your findings are accurate?  How would you continue this laboratory exploration?

 

EDUCATIONAL STANDARDS

USED and / or MET

 

Content Standard A: Science As Inquiry

A1: Abilities necessary to do scientific inquiry:

  • Identify questions and concepts that guide scientific investigations
  • Design and conduct a scientific investigation
  • Use technology and mathematics to improve investigations and communications
  • Formulate and revise scientific explanations and models using logic and evidence
  • Recognize and analyze alternative explanations and models
  • Communicate and defend a scientific argument

 

A2: Understanding about scientific inquiry:

  • Scientists usually inquire about how physical systems function
  • Scientist conduct investigations for a wide variety of reasons
  • Scientists rely on technology to enhance the gathering and manipulation of data
  • Mathematics is essential in scientific inquiry
  • Scientific explanations must adhere to criteria such as a proposed explanation must be logically consistent; it must abide by the rules of evidence; it must be open to questions and possible modifications; and it must be based on historical and current scientific knowledge
  • Results of scientific inquiry emerge from different types of investigations and public communications among scientists

 

Content Standard B: Physical Science

B2: Structure and properties of matter

 

Content Standard G: Science as Inquiry

G1. Science as a human endeavor:

  • Individuals and teams have contributed and will continue to contribute to the scientific enterprise
  • Scientists have ethical traditions
  • Scientists are influenced by societal, cultural, and personal beliefs and ways of viewing the world

 

G2. Nature of scientific knowledge

  • Science distinguishes itself from other ways of knowing and from other bodies of knowledge
  • Scientific explanations must meet certain criteria
  • Because all scientific ideas depend on experimental and observational confirmation, all scientific knowledge is, in principle, subject to change as new evidence becomes available

 

 

 

 

 

 

 

 

 

 

Carnegie Mellon nnnn

NSF Grant DMR 0520425

High School Teachers Summer Internship

 

 

 

 

 

 

 

Other Data- Experimental Results

 

Blkgrn       3386.5        3114.1 3284.5

ubtgrn         1098          1085.9 569.13

whtgrn         750.33      853.69 782.6

Whtgrnlg    488.59       775.83 595.97

blkmrb        1926.1      1783.9 1214.7

Whtmrb      617.45       546.31 702.01

Ylwmrb      1562.4       1681.9 1864.4

ylwmrb 19060  31548  19308

blkmrb             18888  8500    15792

blkgrn               14342  32656  32108

lgwhtgrn             7000  20704  17800

whtgrn                9000  6636    8560

whtmrb   6818  5980    7005

ubtgrn                 6528  7500    8560